典型文献
Theoretical and experimental assessment of a novel method to establish the complete measurement range of the calorimeter and its limit of detection and quantification
文献摘要:
For determining the accuracy of a calorimeter over the instrument's entire measuring range,a novel method has been established.For this new approach,(a)benzoic acid(C6H5CO2H)as a certified reference material(CRM),(b)SiO2 and(c)a mixture of CRM benzoic acid and SiO2 have been used.To illustrate the essential difference between 1)the novel analytical method for control of the entire measurement range and 2)the calorimeter calibration,both applications of benzoic acid(BA)have been demonstrated.An experimental result showed that BA was successfully used to check the whole calorimeter measurement range.The results also showed that the same new method was successfully applied to determine the limit of detection and quantification.A new instrument testing process and a new measurement technique have thus been established.In this way,the cost of using CRM to control the accuracy of measuring the entire measuring range of the calorimeter,as shown in this paper,is minimized.The requirements of the ISO/IEC 17025:2017 standard are satisfied.ISO/IEC 17025:2017,together with ISO 9001:2015(quality management systems),ISO 14001:2015(relate to environmental protection)and ISO 45001:2018(occupational safety),constitute an integrated quality system by which a testing laboratory may also accredit.
文献关键词:
中图分类号:
作者姓名:
Vesna Krsti?
作者机构:
Mining and Metallurgy Institute Bor,Zeleni Bulevar 35,19210 Bor,Serbia;University of Belgrade,Technical Faculty Bor,VJ 12,19210 Bor,Serbia
文献出处:
引用格式:
[1]Vesna Krsti?-.Theoretical and experimental assessment of a novel method to establish the complete measurement range of the calorimeter and its limit of detection and quantification)[J].中国化学工程学报(英文版),2022(04):466-473
A类:
C6H5CO2H,accredit
B类:
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AB值:
0.499332
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