典型文献
Experimental and Data Fitting Guidelines for the Determination of Polymer Crystallization Kinetics
文献摘要：
The crystallization kinetics of semicrystalline polymers is often studied with isothermal experiments and analyzed by fitting the data with analytical expressions of the Avrami and Lauritzen and Hoffman(LH)theories.To correctly carry out the analysis,precautions in both experiments and data fitting should be taken.Here,we systematically discussed the factors that influence the validity of the crystallization kinetics study.The basic concepts and fundamentals of the Avrami and LH theories were introduced at first.Then,experimental protocols were discussed in detail.To clarify the impact of various experimental parameters,selected common polymers,i.e.,polypropylene and polylactide,were studied using various experimental techniques(i.e.,differential scanning calorimetry and polarized light optical microscopy).Common mistakes were simulated under conditions when non-ideal experimental parameters were applied.Furthermore,from a practical point of view,we show how to fit the experimental data to the Avrami and the LH theories,using an Origin? App developed by us.
文献关键词：
中图分类号：
作者姓名：
Ricardo Arpad Pérez-Camargo;Guo-Ming Liu;Du-Jin Wang;Alejandro J.Müller
作者机构：
Beijing National Laboratory for Molecular Sciences,CAS Key Laboratory of Engineering Plastics,Institute of Chemistry,Chinese Academy of Sciences,Beijing 100190,China;University of Chinese Academy of Sciences,Beijing 100049,China;POLYMAT and Department of Polymers and Advanced Materials:Physics,Chemistry and Technology,Faculty of Chemistry,University of the Basque Country UPV/EHU,Donostia-San Sebastián 20018,Spain;IKERBASQUE,Basque Foundation for Science,Bilbao 48013,Spain
文献出处：
引用格式：
[1]Ricardo Arpad Pérez-Camargo;Guo-Ming Liu;Du-Jin Wang;Alejandro J.Müller-.Experimental and Data Fitting Guidelines for the Determination of Polymer Crystallization Kinetics)[J].高分子科学（英文版）,2022(06):658-691
A类：
semicrystalline,Lauritzen,polylactide
B类：
Experimental,Data,Fitting,Guidelines,Determination,Polymer,Crystallization,Kinetics,crystallization,kinetics,polymers,often,studied,isothermal,experiments,analyzed,by,fitting,data,analytical,expressions,Avrami,Hoffman,LH,theories,To,correctly,carry,out,analysis,precautions,both,should,be,taken,Here,systematically,discussed,factors,that,influence,validity,study,basic,concepts,fundamentals,were,introduced,first,Then,experimental,protocols,detail,clarify,impact,various,parameters,selected,common,polypropylene,using,techniques,differential,scanning,calorimetry,polarized,light,optical,microscopy,Common,mistakes,simulated,under,conditions,when,ideal,applied,Furthermore,from,practical,point,view,show,Origin,App,developed
AB值：
0.60802
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