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典型文献
Measuring the Interfacial Thickness of Immiscible Polymer Blends by Nano-probing of Atomic Force Microscopy
文献摘要:
Immiscible polymer blends are an important family of polymer materials.The interfacial thickness between different phases is a very important parameter that dictates,to a great extent,the morphology and properties of such a blend.This work explores and optimizes an up-to-date atomic force microscopy(AFM)of type NanoIR2TM system in order to quantitatively measure the interfacial thickness of immiscible polymer blends.This system is equipped with two nano-probes capable of detecting the response of a material to an infrared pulse called AFM-infrared spectroscopy mode(AFM-IR)or conducting resonance called AFM-Lorentz Contact Resonance mode(AFM-LCR),respectively.Its potential for quantitatively measuring the interfacial thickness of immiscible polymer blends is evaluated using blends composed of polyamide 6(PA6)and polyolefin elastomer(POE)in the presence or absence of a POE containing maleic anhydride(POE-g-MAH)as a compatibilizer.Surface roughness affects adversely the signal intensity and consequently an accurate measurement of the interfacial thickness.Optimum sample surface preparation procedures are proposed.
文献关键词:
作者姓名:
Tian-Tian Li;Si-Bo Cheng;Lian-Fang Feng;Xue-Ping Gu;Cai-Liang Zhang;Guo-Hua Hu
作者机构:
State Key Laboratory of Chemical Engineering,College of Chemical and Biological Engineering,Zhejiang University,Hangzhou 310027,China;Institute of Zhejiang University-Quzhou,Quzhou 324000,China;CNRS-Université de Lorraine,Laboratoire Réactions et Génie des Procédés(LRGP,CNRS UMR 7274),1 rue Grandville,BP20451,54001 Nancy,France
引用格式:
[1]Tian-Tian Li;Si-Bo Cheng;Lian-Fang Feng;Xue-Ping Gu;Cai-Liang Zhang;Guo-Hua Hu-.Measuring the Interfacial Thickness of Immiscible Polymer Blends by Nano-probing of Atomic Force Microscopy)[J].高分子科学(英文版),2022(04):421-430
A类:
Immiscible,NanoIR2TM,polyolefin,compatibilizer
B类:
Measuring,Interfacial,Thickness,Polymer,Blends,by,probing,Atomic,Force,Microscopy,polymer,blends,important,family,materials,interfacial,thickness,between,different,phases,very,parameter,that,dictates,great,extent,morphology,properties,such,This,work,explores,optimizes,up,date,atomic,force,microscopy,AFM,type,system,order,quantitatively,immiscible,equipped,two,nano,probes,capable,detecting,response,infrared,pulse,called,spectroscopy,mode,conducting,resonance,Lorentz,Contact,Resonance,LCR,respectively,Its,potential,measuring,evaluated,using,composed,polyamide,PA6,elastomer,POE,presence,absence,containing,maleic,anhydride,MAH,Surface,roughness,affects,adversely,signal,intensity,consequently,accurate,measurement,Optimum,sample,surface,preparation,procedures,proposed
AB值:
0.606476
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