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典型文献
Optimization of Solid-Phase Extraction Conditions for Perfluorooctanoic Acid in Leachate
文献摘要:
In order to optimize the solid phase extraction(SPE)conditions of perfluorooctanoic acid(PFOA)in the raw leachate and treated leachate,the effects of activator properties,SPE car-tridge,pH value,ionic strength,and eluent properties were stud-ied through single factor experiments.The optimal results of each single factor were obtained.Considering that the concentration of PFOA in the treated leachate is lower than that of the raw leach-ate,the SPE conditions of the treated leachate have been further optimized.Based on the above single-factor experiment,the main influencing factors were screened out as the volume of activator,ionic strength,and volume of eluent,and the three-factor three-level response surface methodology(RSM)was optimized.The optimum SPE conditions of PFOA from treated landfill leachate were as follows:Activation of weak anion exchange(WAX)car-tridge with 10 mL methanol,dosage of 600 mg KC1,6 mL 1%am-monia methanol eluted PFOA,the theory recovery rate is over 95.67%.It has been verified that the error between the predicted value and the actual extraction recovery is small and has good re-peatability.
文献关键词:
作者姓名:
WANG Ying;ZENG Xiaolan;YU Zhipeng;JIN Jiyuan;Mi Ruidong;SUN Yuan
作者机构:
Power China Chengdu Engineering Corporation Limited,Chengdu 610072,Sichuan,China;College of Environment and Ecology,Chongqing University,Chongqing 400045,China
引用格式:
[1]WANG Ying;ZENG Xiaolan;YU Zhipeng;JIN Jiyuan;Mi Ruidong;SUN Yuan-.Optimization of Solid-Phase Extraction Conditions for Perfluorooctanoic Acid in Leachate)[J].武汉大学自然科学学报(英文版),2022(04):341-348
A类:
Perfluorooctanoic,Leachate,tridge,eluent,peatability
B类:
Optimization,Solid,Phase,Extraction,Conditions,Acid,In,order,solid,phase,extraction,SPE,conditions,perfluorooctanoic,acid,PFOA,raw,leachate,treated,effects,activator,properties,car,value,ionic,strength,were,stud,through,single,experiments,optimal,results,obtained,Considering,that,concentration,is,lower,have,been,further,optimized,Based,above,main,influencing,factors,screened,out,volume,three,level,response,surface,methodology,RSM,was,optimum,from,landfill,follows,Activation,weak,anion,exchange,WAX,methanol,dosage,KC1,am,monia,eluted,theory,recovery,rate,It,verified,error,between,predicted,actual,small,good
AB值:
0.487057
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